A novel approach of accurately evaluating residual stress and microstructure of welded electrical steels

In the present research work the determination of residual stress distribution in welded non-oriented electrical steel samples is discussed. Tungsten inert gas was used for the welding method. Residual stress was directly determined through deformation measurements and appropriate math calculations. Two methods were used: the magnetic, non-destructive method of Barkhausen noise and the semi-destructive method of X-ray diffraction. In order to evaluate the accuracy and reliability of the magnetic method applied, the steel samples were subjected to both compressive and tensile stresses and the magnetic noise values were correlated to residual stress values through an appropriate calibration curve. The results were then verified by the XRD method and were further evaluated by examining the microstructure and the mechanical properties of the as received and welded samples through scanning electron microscopy and hardness measurements, respectively. It was found that the deviation between the two methods was within acceptable limits, thus implying potential applicability of the MBN method in non-destructive testing of materials.     

新疆某铀矿淡化少试剂地浸关键技术和工艺参数现场试验研究

为解决新疆某铀矿床地浸生产中的因地下水矿化度高而容易产生化学堵塞问题,在室内研究基础上,进行淡化少试剂现场浸出试验,得出该工艺的关键技术和最佳参数。结果表明,淡化技术、氧化技术、酸化技术、加助溶剂技术是本工艺的关键技术。控制地下水矿化度小于4g/L、溶解氧浓度250~350mg/L、溶液pH值小于6.9、HCO-3浓度为600mg/L左右为淡化少试剂工艺最佳技术参数。该工艺技术将会对同类铀矿地浸具有参考意义。     

获各琦铜矿铜Ⅱ矿体选矿捕收剂方案探索

针对获各琦铜矿铜Ⅱ矿体赋存特点为沉积变质矿床,具有层位控矿及岩性控矿的特点,铜矿体赋存在石英岩中,并由多条矿体组成,存在较大的选矿难度。笔者通过不同药剂制度下进行了选矿指标必选,获得了较优的选矿指标,可提高Cu回收率3%-5%。     

高铋粗铅电解精炼生产控制条件浅析及实践

分析了铋在粗铅电解精炼中的行为,介绍了高铋粗铅电解精炼中存在的问题,通过采取合理搭配粗铅、控制电流密度及电解液成分、阳极泥洗水铅铋置换等有效措施,确保了铅电解生产平稳运行,析出铅合格。     

空气中甲醛含量测试在线监测仪验证

本文依据国标GB/T 18204.26-2000采用酚试剂法测空气中甲醛含量,通过对相同的样品测试,比较采用此方法与市售甲醛在线检测仪AL4021所得数据,验证在线监测仪可靠性。AL4021在高中低(1.5 mg/m3、0.1mg/m3、0.01mg/m3)三个浓度点的测试结果偏差分别为5.47%、14.05%、-3.14%,不超过15%,表明其数据可靠性高,此设备在其标称应用范围内可用。     

基于Kriging代理模型的注塑件残余应力优化分析

以注塑成型制品中脱模后的最大Mises-Hencky残余应力为目标函数,运用基于Kriging代理模型及EI加点准则的序列优化方法,对聚碳酸酯材料制品进行了工艺参数(包括熔体温度、模具温度、注射速率、保压压力及保压时间)优化。算例结果表明,所提出方法可以有效地降低注塑件内的最大Mises-Hencky残余应力。在此基础上对充填阶段进行深入分析,用贝塞尔曲线控制方式代替常规的常速率充填控制方式,进一步降低了制件内的残余应力。     

The Effects of Environmental Temperature and Additional Pressure on the Bonding Characteristics of Co-cured Carbon/Epoxy-Aluminum Single Lap Joints

The aim of this study was to investigate the bonding characteristics of a filament wound structure with an aluminum mandrel under different temperature conditions. During the filament winding process, the filament tension generates pressure in the pre-wound plies and mandrel. To simulate pressure in the filament wound structure with a single lap joint specimen, a pressure-generating device has been introduced and applied to the bonding part of the specimen. The single lap joint, composed of a carbon/epoxy prepreg and aluminum beam, was fabricated by an autoclave degassing molding process, at a pressure of 0.7 MPa (absolute including vacuum) and maximum curing temperature of 135°C. The environmental temperature conditions of ?20°C, 25°C, and 50°C were used in the experimental tests, in order to consider the service condition of passenger cars. The static bonding strength and fatigue life of the specimen under different temperature conditions with and without the additional pressures were measured and compared.     

玉米细菌性枯萎病菌纳米磁标记免疫层析检测试剂与试纸条

分别以粒径为50和100 nm的羧基化纳米磁珠,通过碳二亚胺(EDC)/N-羟基琥珀酰亚胺(NHS)交联法使磁珠与抗体偶联,制备出可特异性识别玉米细菌性枯萎病菌的两种纳米免疫磁珠试剂。基于双抗体夹心法,经实验条件优化,选用100 nm的羧基化纳米磁珠为磁标记探针,组装了玉米细菌性枯萎病菌磁标记免疫层析检测试纸条。该方法用于玉米种子中玉米细菌性枯萎病菌的检测,检出限为1.0×106CFU/m L,15 min内可通过肉眼判读结果,也可用超顺磁共振检测仪实现量化检测,具有简便、快速、现场化检测的优势。     

科研用预制试剂COD消解液的配制研究

以自配消解液代替成本较高的HACH专用试剂,采用分光光度法测定污水中的COD浓度。试验结果表明,用自制的COD消解液在HACH仪器上作出标准曲线,测得的相对误差为0.2%~1.5%,COD浓度值在国家标准质量控制要求范围(±5%)内,无显著性差异,适用于污水中COD浓度的测定。     

以溴酸根插层锌铝水滑石为载体构建新溴源体系

以溴酸根插层锌铝水滑石(Zn/Al-Br O3–-LDHs)为载体,与Br-等还原剂构建形成新型溴源体系。为实现溴源体系在实际应用中的有效控溴,对Zn/Al-Br O3–-LDHs中Br O3–的释放行为进行了研究,并考察了温度、交换离子类型、p H值等因素对Br O3–释放行为的影响。结果表明:升高温度会加快Br O3–的释放,交换离子的交换性越强,Br O3–释放得越快,在p H值为9.0的磷酸盐缓冲溶液中的释放速率要比在p H值为4.0的磷酸盐缓冲溶液中快。采用4种动力学模型对水滑石中Br O3–的释放过程进行动力学拟合,结果表明:LDHs-Br O3–中Br O3–的释放行为符合Bhaskar方程,属粒内扩散控制过程。用LDHs-Br O3–/Br–构建的溴源体系合成了3,5-二溴-2-氨基苯甲酸甲酯,收率为94.7%,纯度为99.8%。